subject:(Diazo)

Michigan State University

1. Guan, Yong (Ph.D.). Construction of a vaulted biaryl ligand library for the aziridination reaction.

Degree: 2012, Michigan State University

URL: http://etd.lib.msu.edu/islandora/object/etd:1798

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Thesis Ph. D. Michigan State University, Chemistry 2012.

A highly enantioselective asymmetric catalytic synthesis of alkynyl aziridines can be achieved from alkynyl imines with diazo… (more)

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Thesis Ph. D. Michigan State University, Chemistry 2012.

A highly enantioselective asymmetric catalytic synthesis of alkynyl aziridines can be achieved from alkynyl imines with diazo compounds mediated by a chiral boroxinate (BOROX) catalyst generated from VANOL or VAPOL ligand. In contrast to the aziridination reaction (AZ reaction) with aryl and alkyl substituted imines, alkynyl imines react to give cis-substituted aziridines with both diazo esters and diazo acetamides. Unexpectedly, the two diazo compounds afford different enantiomers of the cis-aziridine from the same enantiomer of the catalyst. The (S)-BOROX catalyst promotes the reaction of ethyl diazoacetate such that reaction occurs with the Si-face of the imine and the Si-face of the diazo compound. However, in the case of a diazo acetamide, the (S)-BOROX catalyst switches the facial selectivity for reaction of both substrates from Si-face to Re-face. A diverse family of chiral boroxinate Brønsted acids is generated from a library of thirty-one VANOL derivatives that are substituted in the 7,7'-positions. A direct and convergent synthetic access to the ligand library is made viable by a cycloaddition/electrocylization cascade from various p-substituted phenyl acetic acids. The family of ligands is used to screen the catalytic asymmetric AZ reaction of two different benzhydryl imines, one from an aryl aldehyde and the other from an aliphatic aldehyde. Remarkably, the highest asymmetric induction for each substrate was recorded with the same ligand, 7,7'-di-t-butylVANOL. This ligand was in turn screened with a set of 10 different benzhydryl imines to find that this ligand gives an average of 97% ee over all ten imines whereas the corresponding unsubstituted ligand VANOL gives an average of 87% ee and the VAPOL ligand gives an average of 86% ee. Three sets of VANOL ligands: 1) naphthalene skeleton modified; 2) C3-aryl group modified; 3) C1-symmetric VANOL derivatives were synthesized and evaluated in the AZ reaction. Those modifications lead to complicated outcomes. Generally, 7,7'-substituents are beneficial to the AZ reaction, whereas 4,4'- or 8,8'-substituents are detrimental to the AZ reaction. Modification of the C3-aryl effects the enantioselectivity to some extent. Four VAPOL derivatives were prepared and evaluated in the AZ reaction. In addition to the AZ reaction, those VANOL and VAPOL derivatives were evaluated in the reduction of 2-quinolines and VAPOL was found to be the optimal ligand. A novel DMAP-squaramide catalyst was prepared from BINAM and evaluated in the Michael addition of a nitroalkane to a nitroalkene.

Description based on online resource; title from PDF t.p. (ProQuest, viewed on Oct. 7, 2013)

Advisors/Committee Members: Wulff, William D, Maleczka, Robert E, Borhan, Babak, Smith, Milton R.

Subjects/Keywords: Diazo compounds; Chemistry

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APA (6^th Edition):

Guan, Y. (. D. ). (2012). Construction of a vaulted biaryl ligand library for the aziridination reaction. (Thesis). Michigan State University. Retrieved from http://etd.lib.msu.edu/islandora/object/etd:1798

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Guan, Yong (Ph D ). “Construction of a vaulted biaryl ligand library for the aziridination reaction.” 2012. Thesis, Michigan State University. Accessed January 20, 2021. http://etd.lib.msu.edu/islandora/object/etd:1798.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Guan, Yong (Ph D ). “Construction of a vaulted biaryl ligand library for the aziridination reaction.” 2012. Web. 20 Jan 2021.

Vancouver:

Guan Y(D). Construction of a vaulted biaryl ligand library for the aziridination reaction. [Internet] [Thesis]. Michigan State University; 2012. [cited 2021 Jan 20]. Available from: http://etd.lib.msu.edu/islandora/object/etd:1798.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Guan Y(D). Construction of a vaulted biaryl ligand library for the aziridination reaction. [Thesis]. Michigan State University; 2012. Available from: http://etd.lib.msu.edu/islandora/object/etd:1798

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Oregon State University

2. Engebrecht, Ronald Henry. Mechanisms of internal substitution reactions.

Degree: PhD, Chemistry, 1964, Oregon State University

URL: http://hdl.handle.net/1957/48466

Subjects/Keywords: Diazo reaction

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APA (6^th Edition):

Engebrecht, R. H. (1964). Mechanisms of internal substitution reactions. (Doctoral Dissertation). Oregon State University. Retrieved from http://hdl.handle.net/1957/48466

Chicago Manual of Style (16^th Edition):

Engebrecht, Ronald Henry. “Mechanisms of internal substitution reactions.” 1964. Doctoral Dissertation, Oregon State University. Accessed January 20, 2021. http://hdl.handle.net/1957/48466.

MLA Handbook (7^th Edition):

Engebrecht, Ronald Henry. “Mechanisms of internal substitution reactions.” 1964. Web. 20 Jan 2021.

Vancouver:

Engebrecht RH. Mechanisms of internal substitution reactions. [Internet] [Doctoral dissertation]. Oregon State University; 1964. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/1957/48466.

Council of Science Editors:

Engebrecht RH. Mechanisms of internal substitution reactions. [Doctoral Dissertation]. Oregon State University; 1964. Available from: http://hdl.handle.net/1957/48466

Hong Kong University of Science and Technology

3. Ding, Yao. Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene.

Degree: 2015, Hong Kong University of Science and Technology

URL: http://repository.ust.hk/ir/Record/1783.1-78891 ; https://doi.org/10.14711/thesis-b1514646 ; http://repository.ust.hk/ir/bitstream/1783.1-78891/1/th_redirect.html

► Atomic registry of bilayer graphene can significantly modify their electronic structure and properties. In our work, the experimental observation of the electron transfer chemistry on… (more)

Subjects/Keywords: Graphene ; Spectra ; Synthesis ; Diazo compounds

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APA (6^th Edition):

Ding, Y. (2015). Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene. (Thesis). Hong Kong University of Science and Technology. Retrieved from http://repository.ust.hk/ir/Record/1783.1-78891 ; https://doi.org/10.14711/thesis-b1514646 ; http://repository.ust.hk/ir/bitstream/1783.1-78891/1/th_redirect.html

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Ding, Yao. “Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene.” 2015. Thesis, Hong Kong University of Science and Technology. Accessed January 20, 2021. http://repository.ust.hk/ir/Record/1783.1-78891 ; https://doi.org/10.14711/thesis-b1514646 ; http://repository.ust.hk/ir/bitstream/1783.1-78891/1/th_redirect.html.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Ding, Yao. “Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene.” 2015. Web. 20 Jan 2021.

Vancouver:

Ding Y. Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene. [Internet] [Thesis]. Hong Kong University of Science and Technology; 2015. [cited 2021 Jan 20]. Available from: http://repository.ust.hk/ir/Record/1783.1-78891 ; https://doi.org/10.14711/thesis-b1514646 ; http://repository.ust.hk/ir/bitstream/1783.1-78891/1/th_redirect.html.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Ding Y. Angle-dependent reactivity for the chemical modification by diazonium salts on bilayer graphene. [Thesis]. Hong Kong University of Science and Technology; 2015. Available from: http://repository.ust.hk/ir/Record/1783.1-78891 ; https://doi.org/10.14711/thesis-b1514646 ; http://repository.ust.hk/ir/bitstream/1783.1-78891/1/th_redirect.html

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Michigan State University

4. Chi, Frank Kang, 1941-. Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical.

Degree: PhD, Department of Chemistry, 1972, Michigan State University

URL: http://etd.lib.msu.edu/islandora/object/etd:34255

Subjects/Keywords: Diazo compounds

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APA (6^th Edition):

Chi, Frank Kang, 1. (1972). Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical. (Doctoral Dissertation). Michigan State University. Retrieved from http://etd.lib.msu.edu/islandora/object/etd:34255

Chicago Manual of Style (16^th Edition):

Chi, Frank Kang, 1941-. “Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical.” 1972. Doctoral Dissertation, Michigan State University. Accessed January 20, 2021. http://etd.lib.msu.edu/islandora/object/etd:34255.

MLA Handbook (7^th Edition):

Chi, Frank Kang, 1941-. “Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical.” 1972. Web. 20 Jan 2021.

Vancouver:

Chi, Frank Kang 1. Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical. [Internet] [Doctoral dissertation]. Michigan State University; 1972. [cited 2021 Jan 20]. Available from: http://etd.lib.msu.edu/islandora/object/etd:34255.

Council of Science Editors:

Chi, Frank Kang 1. Vibrational spectra of diazopropyne and its photolysis product : the proparglyene radical. [Doctoral Dissertation]. Michigan State University; 1972. Available from: http://etd.lib.msu.edu/islandora/object/etd:34255

Michigan State University

5. Naito, Hiroshi. A study of the decomposition of Diazo-compounds.

Degree: MS, 1919, Michigan State University

URL: http://etd.lib.msu.edu/islandora/object/etd:48980

Subjects/Keywords: Diazo compounds

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APA (6^th Edition):

Naito, H. (1919). A study of the decomposition of Diazo-compounds. (Masters Thesis). Michigan State University. Retrieved from http://etd.lib.msu.edu/islandora/object/etd:48980

Chicago Manual of Style (16^th Edition):

Naito, Hiroshi. “A study of the decomposition of Diazo-compounds.” 1919. Masters Thesis, Michigan State University. Accessed January 20, 2021. http://etd.lib.msu.edu/islandora/object/etd:48980.

MLA Handbook (7^th Edition):

Naito, Hiroshi. “A study of the decomposition of Diazo-compounds.” 1919. Web. 20 Jan 2021.

Vancouver:

Naito H. A study of the decomposition of Diazo-compounds. [Internet] [Masters thesis]. Michigan State University; 1919. [cited 2021 Jan 20]. Available from: http://etd.lib.msu.edu/islandora/object/etd:48980.

Council of Science Editors:

Naito H. A study of the decomposition of Diazo-compounds. [Masters Thesis]. Michigan State University; 1919. Available from: http://etd.lib.msu.edu/islandora/object/etd:48980

University of Arizona

6. Tschampel, Paul, 1936-. The reactions of diazonium salts with a tertiary alcohol .

Degree: 1959, University of Arizona

URL: http://hdl.handle.net/10150/319270

Subjects/Keywords: Diazo compounds.

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APA (6^th Edition):

Tschampel, Paul, 1. (1959). The reactions of diazonium salts with a tertiary alcohol . (Masters Thesis). University of Arizona. Retrieved from http://hdl.handle.net/10150/319270

Chicago Manual of Style (16^th Edition):

Tschampel, Paul, 1936-. “The reactions of diazonium salts with a tertiary alcohol .” 1959. Masters Thesis, University of Arizona. Accessed January 20, 2021. http://hdl.handle.net/10150/319270.

MLA Handbook (7^th Edition):

Tschampel, Paul, 1936-. “The reactions of diazonium salts with a tertiary alcohol .” 1959. Web. 20 Jan 2021.

Vancouver:

Tschampel, Paul 1. The reactions of diazonium salts with a tertiary alcohol . [Internet] [Masters thesis]. University of Arizona; 1959. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/10150/319270.

Council of Science Editors:

Tschampel, Paul 1. The reactions of diazonium salts with a tertiary alcohol . [Masters Thesis]. University of Arizona; 1959. Available from: http://hdl.handle.net/10150/319270

Michigan State University

7. Au, Andrew Tai Chiu. Investigaiton of potential routes to 1, 5-diazonene.

Degree: MS, Dept. of Chemistry, 1968, Michigan State University

URL: http://etd.lib.msu.edu/islandora/object/etd:10843

Subjects/Keywords: Diazo compounds

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APA (6^th Edition):

Au, A. T. C. (1968). Investigaiton of potential routes to 1, 5-diazonene. (Masters Thesis). Michigan State University. Retrieved from http://etd.lib.msu.edu/islandora/object/etd:10843

Chicago Manual of Style (16^th Edition):

Au, Andrew Tai Chiu. “Investigaiton of potential routes to 1, 5-diazonene.” 1968. Masters Thesis, Michigan State University. Accessed January 20, 2021. http://etd.lib.msu.edu/islandora/object/etd:10843.

MLA Handbook (7^th Edition):

Au, Andrew Tai Chiu. “Investigaiton of potential routes to 1, 5-diazonene.” 1968. Web. 20 Jan 2021.

Vancouver:

Au ATC. Investigaiton of potential routes to 1, 5-diazonene. [Internet] [Masters thesis]. Michigan State University; 1968. [cited 2021 Jan 20]. Available from: http://etd.lib.msu.edu/islandora/object/etd:10843.

Council of Science Editors:

Au ATC. Investigaiton of potential routes to 1, 5-diazonene. [Masters Thesis]. Michigan State University; 1968. Available from: http://etd.lib.msu.edu/islandora/object/etd:10843

Michigan State University

8. Brewbaker, James Lee. Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes.

Degree: PhD, Department of Chemistry, 1968, Michigan State University

URL: http://etd.lib.msu.edu/islandora/object/etd:39414

Subjects/Keywords: Diazo compounds

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APA (6^th Edition):

Brewbaker, J. L. (1968). Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes. (Doctoral Dissertation). Michigan State University. Retrieved from http://etd.lib.msu.edu/islandora/object/etd:39414

Chicago Manual of Style (16^th Edition):

Brewbaker, James Lee. “Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes.” 1968. Doctoral Dissertation, Michigan State University. Accessed January 20, 2021. http://etd.lib.msu.edu/islandora/object/etd:39414.

MLA Handbook (7^th Edition):

Brewbaker, James Lee. “Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes.” 1968. Web. 20 Jan 2021.

Vancouver:

Brewbaker JL. Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes. [Internet] [Doctoral dissertation]. Michigan State University; 1968. [cited 2021 Jan 20]. Available from: http://etd.lib.msu.edu/islandora/object/etd:39414.

Council of Science Editors:

Brewbaker JL. Cyclizations of 1,3-bisdiazopropane and 3-diazopropenes. [Doctoral Dissertation]. Michigan State University; 1968. Available from: http://etd.lib.msu.edu/islandora/object/etd:39414

9. Pons, Amandine. Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes.

Degree: Docteur es, Chimie organique, 2017, Normandie

URL: http://www.theses.fr/2017NORMIR12

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Le motif cyclopropanique est présent dans de nombreux composés bioactifs d'origine naturelle ou non-naturelle auxquels il confère une certaine rigidité structurale, qui permet d'augmenter leur… (more)

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Le motif cyclopropanique est présent dans de nombreux composés bioactifs d'origine naturelle ou non-naturelle auxquels il confère une certaine rigidité structurale, qui permet d'augmenter leur biodisponibilité et leur stabilité métabolique. Par ailleurs, l'atome de fluor possède des propriétés particulières dues entre autres à sa forte électronégativité et sa petite taille. Cela permet de modifier les propriétés physico-chimiques des molécules qui le contiennent, telles que l'acidité, la lipophilie ou encore la solubilité. Par conséquent, les cyclopropanes fluorés représentent des motifs intéressants dans la mesure où ils combinent les propriétés des cyclopropanes et celles de l'atome de fluor. Dans ce contexte, nous nous sommes tout d'abord intéressés à la synthèse énantiosélective de cyclopropanes fluorés polyfonctionnalisés à partir d'oléfines fluorées et de composés diazos, par catalyse au rhodium. Pour cela, deux types de composés diazos ont été utilisés : les diaccepteurs et les donneur-accepteurs. Cette méthodologie a été étendue à la synthèse de cyclopropanes chlorés et bromés. Afin de mettre en valeur les composés ainsi obtenus, nous avons ensuite étudié la synthèse de molécules d'intérêt biologique, et plus précisément de mimes d'aminoacides contenant un cyclopropane fluoré. En effet, leur introduction dans des peptides pourrait permettre d'en modifier la conformation et l'interaction avec les récepteurs biologiques. Dans ce cadre, la synthèse d'un mime de proline contenant un cyclopropane fluoré a été développée. Par ailleurs, un mime de leucine contenant un cyclopropane fluoré a été introduit dans la séquence minimum active de la neurotensine et permet d'obtenir une bonne sélectivité pour le récepteur NTS2, ce qui ouvre des perspectives pour le développement de nouveaux analgésiques possédant moins d'effets secondaires. Pour terminer, nous avons examiné la synthèse de composés diazos en flux continu. A l'heure actuelle, ceux-ci sont peu utilisés dans l'industrie car ils présentent une certaine toxicité, une potentielle explosivité et une instabilité qui limite leur stockage. La chimie en flux continu constitue donc une alternative pour les utiliser, puisque leur synthèse, leur purification et leur mise en réaction se fait en continu sur de petites quantités à la fois et ne nécessite pas d'intervention de la part d'un opérateur. Ainsi, les risques présentés par la montée en échelle de la réaction de cyclopropanation précédemment développée sont fortement diminués.

The cyclopropane ring is present in many natural or non-natural bioactive compounds, whose biodisponibility and metabolic stability is increased by its structural rigidity. Besides, the fluorine atom displays singular properties due to its high electronegativity and its small size. This enables to modify the physico-chemical properties of molecules such as acidity, lipophilicity or solubility. As a consequence, fluorinated cyclopropanes represent interesting scaffolds since they combine the properties of cyclopropanes and fluorine atom. In…

Advisors/Committee Members: Jubault, Philippe (thesis director), Pannecoucke, Xavier (thesis director).

Subjects/Keywords: Composés diazo; Catalyse au rhodium; Fluorine; Diazo compounds; Rhodium catalysis

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APA (6^th Edition):

Pons, A. (2017). Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes. (Doctoral Dissertation). Normandie. Retrieved from http://www.theses.fr/2017NORMIR12

Chicago Manual of Style (16^th Edition):

Pons, Amandine. “Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes.” 2017. Doctoral Dissertation, Normandie. Accessed January 20, 2021. http://www.theses.fr/2017NORMIR12.

MLA Handbook (7^th Edition):

Pons, Amandine. “Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes.” 2017. Web. 20 Jan 2021.

Vancouver:

Pons A. Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes. [Internet] [Doctoral dissertation]. Normandie; 2017. [cited 2021 Jan 20]. Available from: http://www.theses.fr/2017NORMIR12.

Council of Science Editors:

Pons A. Nouvelles méthodes d’accès catalytiques et énantiosélectives aux cyclopropanes fluorés : New catalytic and enantioselective methods to access fluorinated cyclopropranes. [Doctoral Dissertation]. Normandie; 2017. Available from: http://www.theses.fr/2017NORMIR12

University College Cork

10. Buckley, Naomi M. Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential.

Degree: 2013, University College Cork

URL: http://hdl.handle.net/10468/1302

► The research described in this thesis focuses on the design and synthesis of stable α-diazosulfoxides and investigation of their reactivity under a variety of conditions… (more)

▼ The research described in this thesis focuses on the design and synthesis of stable α-diazosulfoxides and investigation of their reactivity under a variety of conditions (transition-metal catalysis, thermal, photochemical and microwave) with a particular emphasis on the synthesis of novel heterocyclic compounds with potential biological activity. The exclusive reaction pathway for these α-diazosulfoxides was found to be hetero-Wolff rearrangement to give α-oxosulfine intermediates. In the first chapter, a literature review of sulfines is presented, including a discussion of naturally occurring sulfines, and an overview of the synthesis and reactivity of sulfines. The potential of sulfines in organic synthesis and recent developments in particular are highlighted. The second chapter discusses the synthesis and reactivity of α-diazosulfoxides, building on earlier results in this research group. The synthesis of lactone-based α-diazosulfoxides and, for the first time, ketone-based benzofused and monocyclic α-diazosulfoxides is described. The reactivity of these α-diazosulfoxides is then explored under a variety of conditions, such as transition-metal catalysis, photochemical and microwave, generating labile α-oxosulfine intermediates, which are trapped using amines and dienes, in addition to the spontaneous reaction pathways which occur with α-oxosulfines in the absence of a trap. A new reaction pathway was explored with the lactone based α-oxosulfines, involving reaction with amines to generate novel 3-aminofuran-2(5H)-ones via carbophilic attack, in very good yields. The reactivity of ketone-based α-diazosulfoxides was explored for the first time, and once again, pseudo-Wolff rearrangement to the α-oxosulfines was the exclusive reaction pathway observed. The intermediacy of the α-oxosulfines was confirmed by trapping as cycloadducts, with the stereochemical features dependant on the reaction conditions. In the absence of a diene trap, a number of reaction fates from the α-oxosulfines were observed, including complete sulfinyl extrusion to give indanones, sulfur extrusion to give indanediones, and, to a lesser extent, dimerisation. The indanediones were characterised by trapping as quinoxalines, to enable full characterisation. One of the overriding outcomes of this thesis was the provision of new insights into the behaviour of α-oxosulfines with different transition metal catalysts, and under thermal, microwave and photolysis conditions. A series of 3-aminofuran-2(5H)-ones and benzofused dihydro-2H-thiopyran S-oxides were submitted for anticancer screening at the U.S. National Cancer Institute. A number of these derivatives were identified as hit compounds, with excellent cell growth inhibition. One 3-aminofuran-2(5H)-one derivative has been chosen for further screening. The third chapter details the full experimental procedures, including spectroscopic and analytical data for the compounds prepared during this research. The data for the crystal structures are contained in the attached CD. Advisors/Committee Members: Collins, Stuart G., Maguire, Anita R., IRCSET.

Subjects/Keywords: Organic synthesis; Diazo chemistry; Reactive intermediates

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APA (6^th Edition):

Buckley, N. M. (2013). Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential. (Thesis). University College Cork. Retrieved from http://hdl.handle.net/10468/1302

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Buckley, Naomi M. “Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential.” 2013. Thesis, University College Cork. Accessed January 20, 2021. http://hdl.handle.net/10468/1302.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Buckley, Naomi M. “Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential.” 2013. Web. 20 Jan 2021.

Vancouver:

Buckley NM. Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential. [Internet] [Thesis]. University College Cork; 2013. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/10468/1302.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Buckley NM. Synthesis and reactivity of α-diazo-β-keto sulfoxides: scope and synthetic potential. [Thesis]. University College Cork; 2013. Available from: http://hdl.handle.net/10468/1302

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Loughborough University

11. Cox, Geoffrey Gale. Investigations towards the reactivity of rhodium bound carbenes.

Degree: PhD, 1993, Loughborough University

URL: http://hdl.handle.net/2134/11950

► A short series of diazo compounds containing a primary alcohol and one or more other carbene traps were synthesised. The result in each case, from… (more)

Subjects/Keywords: 547; Diazo chemistry

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APA (6^th Edition):

Cox, G. G. (1993). Investigations towards the reactivity of rhodium bound carbenes. (Doctoral Dissertation). Loughborough University. Retrieved from http://hdl.handle.net/2134/11950

Chicago Manual of Style (16^th Edition):

Cox, Geoffrey Gale. “Investigations towards the reactivity of rhodium bound carbenes.” 1993. Doctoral Dissertation, Loughborough University. Accessed January 20, 2021. http://hdl.handle.net/2134/11950.

MLA Handbook (7^th Edition):

Cox, Geoffrey Gale. “Investigations towards the reactivity of rhodium bound carbenes.” 1993. Web. 20 Jan 2021.

Vancouver:

Cox GG. Investigations towards the reactivity of rhodium bound carbenes. [Internet] [Doctoral dissertation]. Loughborough University; 1993. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/2134/11950.

Council of Science Editors:

Cox GG. Investigations towards the reactivity of rhodium bound carbenes. [Doctoral Dissertation]. Loughborough University; 1993. Available from: http://hdl.handle.net/2134/11950

Princeton University

12. Gray, Erin Elizabeth. Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion .

Degree: PhD, 2017, Princeton University

URL: http://arks.princeton.edu/ark:/88435/dsp01dr26z089j

► Transition-metal catalysis is an enabling strategy for selective bond formation and activation that has become pervasive in modern synthetic organic chemistry. This dissertation outlines two… (more)

▼ Transition-metal catalysis is an enabling strategy for selective bond formation and activation that has become pervasive in modern synthetic organic chemistry. This dissertation outlines two distinct areas in which we contributed to this field: In Part I, the formulation and implementation of (TMEDA)Ni(o-tolyl)Cl as a new air-stable nickel(II) precatalyst is described. This complex is compatible with a range of reaction conditions and promotes many useful nickel-catalyzed transformations, including various cross-coupling and cyclization reactions. Importantly, the use of TMEDA as a labile supporting ligand enables the exchange with diverse ligand classes, establishing (TMEDA)Ni(o-tolyl)Cl as a modular precatalyst. Investigations into the precatalyst’s activation reveal the mechanism of reduction varies based on the reaction conditions. Evidence supports boron–nickel transmetalation-reductive elimination and nickel–nickel transmetalation-reductive elimination as two possible pathways for activation. Part II of this dissertation focuses on the development of a copper-catalyzed H–F insertion into α-diazocarbonyl compounds. This strategy takes advantage of the rapid reaction of copper with α-diazocarbonyl substrates to generate a copper carbenoid in situ under mild conditions. Nucleophilic fluorination of this intermediate is then achieved using the combination of potassium fluoride and hexafluoroisopropanol as a reactive equivalent of HF. Details of the initial reaction discovery and optimization of the asymmetric transformation are presented, and further studies examining the scope of the racemic counterpart demonstrate the exceptional functional group tolerance of the method. This approach provides access to valuable α-fluorocarbonyl derivatives, which have broad utility as pharmaceuticals and radiotracers. Furthermore, translation of the method to a radiofluorination protocol was accomplished by using [18F]KF, affording an attractive route to 18F-labeled biomolecules for positron emission tomography. Advisors/Committee Members: Doyle, Abigail G (advisor).

Subjects/Keywords: copper; diazo; fluorine; nickel; precatalyst; radiofluorination

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APA (6^th Edition):

Gray, E. E. (2017). Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion . (Doctoral Dissertation). Princeton University. Retrieved from http://arks.princeton.edu/ark:/88435/dsp01dr26z089j

Chicago Manual of Style (16^th Edition):

Gray, Erin Elizabeth. “Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion .” 2017. Doctoral Dissertation, Princeton University. Accessed January 20, 2021. http://arks.princeton.edu/ark:/88435/dsp01dr26z089j.

MLA Handbook (7^th Edition):

Gray, Erin Elizabeth. “Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion .” 2017. Web. 20 Jan 2021.

Vancouver:

Gray EE. Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion . [Internet] [Doctoral dissertation]. Princeton University; 2017. [cited 2021 Jan 20]. Available from: http://arks.princeton.edu/ark:/88435/dsp01dr26z089j.

Council of Science Editors:

Gray EE. Part I. Development of a Modular, Air-Stable Nickel Precatalyst; Part II. Nucleophilic (Radio)Fluorination of α-Diazocarbonyl Compounds Enabled by Copper-Catalyzed H–F Insertion . [Doctoral Dissertation]. Princeton University; 2017. Available from: http://arks.princeton.edu/ark:/88435/dsp01dr26z089j

University of Arizona

13. Langley, Martha Ella, 1933-. The reaction of diazonium sulfates with alcohols .

Degree: 1957, University of Arizona

URL: http://hdl.handle.net/10150/319333

Subjects/Keywords: Diazo compounds.; Alcohol.

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APA (6^th Edition):

Langley, Martha Ella, 1. (1957). The reaction of diazonium sulfates with alcohols . (Masters Thesis). University of Arizona. Retrieved from http://hdl.handle.net/10150/319333

Chicago Manual of Style (16^th Edition):

Langley, Martha Ella, 1933-. “The reaction of diazonium sulfates with alcohols .” 1957. Masters Thesis, University of Arizona. Accessed January 20, 2021. http://hdl.handle.net/10150/319333.

MLA Handbook (7^th Edition):

Langley, Martha Ella, 1933-. “The reaction of diazonium sulfates with alcohols .” 1957. Web. 20 Jan 2021.

Vancouver:

Langley, Martha Ella 1. The reaction of diazonium sulfates with alcohols . [Internet] [Masters thesis]. University of Arizona; 1957. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/10150/319333.

Council of Science Editors:

Langley, Martha Ella 1. The reaction of diazonium sulfates with alcohols . [Masters Thesis]. University of Arizona; 1957. Available from: http://hdl.handle.net/10150/319333

University of Arizona

14. Zolton, Lorraine, 1935-. DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES .

Degree: 1962, University of Arizona

URL: http://hdl.handle.net/10150/284456

Subjects/Keywords: Diazo reaction.; Amines.

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APA (6^th Edition):

Zolton, Lorraine, 1. (1962). DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES . (Doctoral Dissertation). University of Arizona. Retrieved from http://hdl.handle.net/10150/284456

Chicago Manual of Style (16^th Edition):

Zolton, Lorraine, 1935-. “DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES .” 1962. Doctoral Dissertation, University of Arizona. Accessed January 20, 2021. http://hdl.handle.net/10150/284456.

MLA Handbook (7^th Edition):

Zolton, Lorraine, 1935-. “DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES .” 1962. Web. 20 Jan 2021.

Vancouver:

Zolton, Lorraine 1. DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES . [Internet] [Doctoral dissertation]. University of Arizona; 1962. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/10150/284456.

Council of Science Editors:

Zolton, Lorraine 1. DIAZOTIZATION OF ALIPHATIC AND AROMATIC AMINES . [Doctoral Dissertation]. University of Arizona; 1962. Available from: http://hdl.handle.net/10150/284456

The Ohio State University

15. Chang, Sou-Jen. Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry.

Degree: PhD, Graduate School, 1979, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487089582132542

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Chang, S. (1979). Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1487089582132542

Chicago Manual of Style (16^th Edition):

Chang, Sou-Jen. “Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry.” 1979. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487089582132542.

MLA Handbook (7^th Edition):

Chang, Sou-Jen. “Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry.” 1979. Web. 20 Jan 2021.

Vancouver:

Chang S. Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry. [Internet] [Doctoral dissertation]. The Ohio State University; 1979. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487089582132542.

Council of Science Editors:

Chang S. Part I: Thermal and photolytic behavior of diazoacenaphthenone systems; chemistry of acenaphthenequinone bis(p̲-tosylhydrazone). ; Part II: 5-bromo-4-quinolyldiazomethane and 4-quinolyldiazomethane: synthesis, thermolysis and photochemistry. [Doctoral Dissertation]. The Ohio State University; 1979. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487089582132542

The Ohio State University

16. Holton, Terrence Charles,1938-. The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate.

Degree: PhD, Graduate School, 1969, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486663155897603

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Holton, T. C. (1969). The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486663155897603

Chicago Manual of Style (16^th Edition):

Holton, Terrence Charles,1938-. “The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate.” 1969. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486663155897603.

MLA Handbook (7^th Edition):

Holton, Terrence Charles,1938-. “The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate.” 1969. Web. 20 Jan 2021.

Vancouver:

Holton TC. The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate. [Internet] [Doctoral dissertation]. The Ohio State University; 1969. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486663155897603.

Council of Science Editors:

Holton TC. The synthesis of diazo compounds by low-temperature oxidation of hydrazones with lead tetraacetate. [Doctoral Dissertation]. The Ohio State University; 1969. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486663155897603

The Ohio State University

17. Shankar, B. K. Ravi. Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives.

Degree: PhD, Graduate School, 1981, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487156013007639

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Shankar, B. K. R. (1981). Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1487156013007639

Chicago Manual of Style (16^th Edition):

Shankar, B K Ravi. “Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives.” 1981. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487156013007639.

MLA Handbook (7^th Edition):

Shankar, B K Ravi. “Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives.” 1981. Web. 20 Jan 2021.

Vancouver:

Shankar BKR. Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives. [Internet] [Doctoral dissertation]. The Ohio State University; 1981. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487156013007639.

Council of Science Editors:

Shankar BKR. Part I. Chemistry of 6-substituted-5-acenaphthyldiazomethanes and 7-substituted-6-perinaphthyldiazomethanes ; Part II. Rhodium ion catalyzed decomposition of diazo compounds. Part III. Chemistry of 1-diazoacenaphthene derivatives. [Doctoral Dissertation]. The Ohio State University; 1981. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487156013007639

The Ohio State University

18. Shiue, Gong-Huey. Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene.

Degree: PhD, Graduate School, 1983, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487238163206334

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Shiue, G. (1983). Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1487238163206334

Chicago Manual of Style (16^th Edition):

Shiue, Gong-Huey. “Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene.” 1983. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487238163206334.

MLA Handbook (7^th Edition):

Shiue, Gong-Huey. “Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene.” 1983. Web. 20 Jan 2021.

Vancouver:

Shiue G. Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene. [Internet] [Doctoral dissertation]. The Ohio State University; 1983. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487238163206334.

Council of Science Editors:

Shiue G. Photochemical and thermal behaviors of 4-diazopyrazole and 4H?-pyrazolylidene. [Doctoral Dissertation]. The Ohio State University; 1983. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1487238163206334

The Ohio State University

19. Magee, Walter Lee. The chemistry of 3-diazopyrazoles.

Degree: PhD, Graduate School, 1974, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486985327536572

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Magee, W. L. (1974). The chemistry of 3-diazopyrazoles. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486985327536572

Chicago Manual of Style (16^th Edition):

Magee, Walter Lee. “The chemistry of 3-diazopyrazoles.” 1974. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486985327536572.

MLA Handbook (7^th Edition):

Magee, Walter Lee. “The chemistry of 3-diazopyrazoles.” 1974. Web. 20 Jan 2021.

Vancouver:

Magee WL. The chemistry of 3-diazopyrazoles. [Internet] [Doctoral dissertation]. The Ohio State University; 1974. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486985327536572.

Council of Science Editors:

Magee WL. The chemistry of 3-diazopyrazoles. [Doctoral Dissertation]. The Ohio State University; 1974. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486985327536572

The Ohio State University

20. Bailey, Robert Jackson. Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes.

Degree: PhD, Graduate School, 1974, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486986969535875

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Bailey, R. J. (1974). Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486986969535875

Chicago Manual of Style (16^th Edition):

Bailey, Robert Jackson. “Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes.” 1974. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486986969535875.

MLA Handbook (7^th Edition):

Bailey, Robert Jackson. “Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes.” 1974. Web. 20 Jan 2021.

Vancouver:

Bailey RJ. Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes. [Internet] [Doctoral dissertation]. The Ohio State University; 1974. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486986969535875.

Council of Science Editors:

Bailey RJ. Neighboring heteroatom participation in the decomposition of proximally substituted aryldiazomethanes. [Doctoral Dissertation]. The Ohio State University; 1974. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486986969535875

The Ohio State University

21. Fleming, James Charles. Chemistry of the diazooxides : 10-diazoanthrone.

Degree: PhD, Graduate School, 1964, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486566394243784

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Fleming, J. C. (1964). Chemistry of the diazooxides : 10-diazoanthrone. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486566394243784

Chicago Manual of Style (16^th Edition):

Fleming, James Charles. “Chemistry of the diazooxides : 10-diazoanthrone.” 1964. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486566394243784.

MLA Handbook (7^th Edition):

Fleming, James Charles. “Chemistry of the diazooxides : 10-diazoanthrone.” 1964. Web. 20 Jan 2021.

Vancouver:

Fleming JC. Chemistry of the diazooxides : 10-diazoanthrone. [Internet] [Doctoral dissertation]. The Ohio State University; 1964. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486566394243784.

Council of Science Editors:

Fleming JC. Chemistry of the diazooxides : 10-diazoanthrone. [Doctoral Dissertation]. The Ohio State University; 1964. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486566394243784

The Ohio State University

22. Jordan, David Milton. A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones.

Degree: PhD, Graduate School, 1965, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu148656755945309

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Jordan, D. M. (1965). A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu148656755945309

Chicago Manual of Style (16^th Edition):

Jordan, David Milton. “A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones.” 1965. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu148656755945309.

MLA Handbook (7^th Edition):

Jordan, David Milton. “A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones.” 1965. Web. 20 Jan 2021.

Vancouver:

Jordan DM. A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones. [Internet] [Doctoral dissertation]. The Ohio State University; 1965. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu148656755945309.

Council of Science Editors:

Jordan DM. A kinetic investigation of the thermal and acid-catalyzed decompositions of [alpha]-diazoacetophenones. [Doctoral Dissertation]. The Ohio State University; 1965. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu148656755945309

The Ohio State University

23. Lange, Raymond Joseph. An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system.

Degree: PhD, Graduate School, 1966, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486638986097655

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Lange, R. J. (1966). An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system. (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486638986097655

Chicago Manual of Style (16^th Edition):

Lange, Raymond Joseph. “An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system.” 1966. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486638986097655.

MLA Handbook (7^th Edition):

Lange, Raymond Joseph. “An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system.” 1966. Web. 20 Jan 2021.

Vancouver:

Lange RJ. An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system. [Internet] [Doctoral dissertation]. The Ohio State University; 1966. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486638986097655.

Council of Science Editors:

Lange RJ. An approach to a stable carbene : chemistry of the 14H-dibenzo (a,j)-xanthyl system. [Doctoral Dissertation]. The Ohio State University; 1966. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486638986097655

The Ohio State University

24. Kurtz, Donald Ward. The synthesis and reactions of substituted α-diazo imines .

Degree: PhD, Graduate School, 1967, The Ohio State University

URL: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486644760190312

Subjects/Keywords: Chemistry; Diazo compounds

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APA (6^th Edition):

Kurtz, D. W. (1967). The synthesis and reactions of substituted α-diazo imines . (Doctoral Dissertation). The Ohio State University. Retrieved from http://rave.ohiolink.edu/etdc/view?acc_num=osu1486644760190312

Chicago Manual of Style (16^th Edition):

Kurtz, Donald Ward. “The synthesis and reactions of substituted α-diazo imines .” 1967. Doctoral Dissertation, The Ohio State University. Accessed January 20, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486644760190312.

MLA Handbook (7^th Edition):

Kurtz, Donald Ward. “The synthesis and reactions of substituted α-diazo imines .” 1967. Web. 20 Jan 2021.

Vancouver:

Kurtz DW. The synthesis and reactions of substituted α-diazo imines . [Internet] [Doctoral dissertation]. The Ohio State University; 1967. [cited 2021 Jan 20]. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486644760190312.

Council of Science Editors:

Kurtz DW. The synthesis and reactions of substituted α-diazo imines . [Doctoral Dissertation]. The Ohio State University; 1967. Available from: http://rave.ohiolink.edu/etdc/view?acc_num=osu1486644760190312

Simon Fraser University

25. Carroll, James Allen. Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides.

Degree: 1978, Simon Fraser University

URL: http://summit.sfu.ca/item/3095

Subjects/Keywords: Diazo compounds.; Diazo reaction.; Transition metal compounds.; Complex ions.

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APA (6^th Edition):

Carroll, J. A. (1978). Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides. (Thesis). Simon Fraser University. Retrieved from http://summit.sfu.ca/item/3095

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Carroll, James Allen. “Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides.” 1978. Thesis, Simon Fraser University. Accessed January 20, 2021. http://summit.sfu.ca/item/3095.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Carroll, James Allen. “Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides.” 1978. Web. 20 Jan 2021.

Vancouver:

Carroll JA. Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides. [Internet] [Thesis]. Simon Fraser University; 1978. [cited 2021 Jan 20]. Available from: http://summit.sfu.ca/item/3095.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Carroll JA. Complexes of aryldiazene and arylhydrazide : products of the reactions of benzenediazonium ions with transition metal hydrides. [Thesis]. Simon Fraser University; 1978. Available from: http://summit.sfu.ca/item/3095

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Universidade Estadual de Campinas

26. Augusti, Rodinei. Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas.

Degree: 1993, Universidade Estadual de Campinas

URL: http://repositorio.unicamp.br/jspui/handle/REPOSIP/250110

Subjects/Keywords: Orbitais moleculares; Compostos de diazo

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APA (6^th Edition):

Augusti, R. (1993). Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas. (Thesis). Universidade Estadual de Campinas. Retrieved from http://repositorio.unicamp.br/jspui/handle/REPOSIP/250110

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Augusti, Rodinei. “Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas.” 1993. Thesis, Universidade Estadual de Campinas. Accessed January 20, 2021. http://repositorio.unicamp.br/jspui/handle/REPOSIP/250110.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Augusti, Rodinei. “Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas.” 1993. Web. 20 Jan 2021.

Vancouver:

Augusti R. Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas. [Internet] [Thesis]. Universidade Estadual de Campinas; 1993. [cited 2021 Jan 20]. Available from: http://repositorio.unicamp.br/jspui/handle/REPOSIP/250110.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Augusti R. Desenvolvimento de um metodo novo e geral de sintese de 1, 2, 3-triazois a partir do estudo da reatividade de compostos diazoisatinicos frente a enaminonas. [Thesis]. Universidade Estadual de Campinas; 1993. Available from: http://repositorio.unicamp.br/jspui/handle/REPOSIP/250110

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

University of Delaware

27. Selvaraj, Ramajeyam. Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity.

Degree: PhD, University of Delaware, Department of Chemistry and Biochemistry, 2014, University of Delaware

URL: http://udspace.udel.edu/handle/19716/16780

► This dissertation has been focused on the development of new synthetic methods for carbometallation and in the use of rapid bioorthgonal chemistry to construct 18… (more)

▼ This dissertation has been focused on the development of new synthetic methods for carbometallation and in the use of rapid bioorthgonal chemistry to construct 18 F-PET probes for nuclear medicine. While the canon of Rh(II)-catalyzed reactions with diazo compounds is extensive, there were no reports in which organometallic compounds have been engaged as substrates. Organozinc reagents have been employed in a variety of transition-metal catalyzed coupling reactions, and have been shown to display a wide range of functional group tolerance. In Chapter 1, it is shown that organozinc reagents may participate in reactions with diazo compounds by two distinct, catalyst-dependent mechanisms. With Rh 2 (DIEA)4 , the likely reaction mechanism initial formation of a Rh-carbene and subsequent carbozincation to give a zinc enolate. With Rh2 (OAc)4 , initial formation of an azine preceeds a subsequent 1,2-addition reaction with an organozinc reagent. This straightforward route to the hydrazone products provides a useful method for preparing chiral quaternary α-aminoesters or pyrazoles via the Knorr condensation with 1,3-diketones. Crossover and deuterium labeling experiments provide evidence for the mechanisms proposed. 1,2,4,5-Tetrazines, or s -tetrazines, have a rich history that bridges applications in synthesis, energetic materials, supramolecular chemistry and bioorthogonal chemistry. Tetrazines are almost always prepared through the initial formation and then oxidation of 1,4-dihydro-s -tetrazines. Nitrous reagents are commonly used as the oxidant for 1,4-dihydro-s -tetrazine oxidation. The advantage of using nitrous acid is the low cost of the reagent. A disadvantage of nitrous acid is that of functional group tolerance due to the acidic and harshly oxidizing conditions. In Chapter 2, it is described that phenyliodonium diacetate serves as a mild and efficient reagent for converting dihydro- s -tetrazines to s -tetrazine derivatives. This oxidant provided an efficient, large-scale synthesis of an s -tetrazine derivative that is used in various applications in nuclear medicine and cell labeling. Exploration of substrate scope showed that heterocycles like furan and pyridine are tolerated, and that dialkyl and diphenyl substitutions are also tolerated. In Chapter 3, it is shown that tetrazine-trans -cycloctene ligation can be used efficiently for Positron Emission Tomography (PET) probe construction. The fast reaction rate for the tetrazine-trans -cycloctene ligation is shown to be advantageous for achieving labeling at low concentration and with a minimal excess of substrate, reducing the effects of competitive inhibition from the unlabeled substrate. An initially developed system based on dipyridyl-s-tetrazine was successfully used for rapid construction of an 18 F-labeled cRGD conjugate that could be used for in vivo imaging in a mouse tumor model. However, metabolic stability studies showed that the probe stability was only modest. A CF3-substituted 3,6-diphenyl-s-tetrazine derivative displays fast conjugation rates… Advisors/Committee Members: Fox, Joseph M..

Subjects/Keywords: Tomography, Emission.; Carbon.; Zinc.; Diazo compounds.; Esters.; Reactivity (Chemistry); Tetrazine.; Catalysis.

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APA (6^th Edition):

Selvaraj, R. (2014). Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity. (Doctoral Dissertation). University of Delaware. Retrieved from http://udspace.udel.edu/handle/19716/16780

Chicago Manual of Style (16^th Edition):

Selvaraj, Ramajeyam. “Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity.” 2014. Doctoral Dissertation, University of Delaware. Accessed January 20, 2021. http://udspace.udel.edu/handle/19716/16780.

MLA Handbook (7^th Edition):

Selvaraj, Ramajeyam. “Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity.” 2014. Web. 20 Jan 2021.

Vancouver:

Selvaraj R. Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity. [Internet] [Doctoral dissertation]. University of Delaware; 2014. [cited 2021 Jan 20]. Available from: http://udspace.udel.edu/handle/19716/16780.

Council of Science Editors:

Selvaraj R. Catalytic carbozincation of diazoesters and development of probes for F-18 imaging based on rapid bioorthogonal reactivity. [Doctoral Dissertation]. University of Delaware; 2014. Available from: http://udspace.udel.edu/handle/19716/16780

Hong Kong University of Science and Technology

28. Ding, Yao CBME. Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials.

Degree: 2018, Hong Kong University of Science and Technology

URL: http://repository.ust.hk/ir/Record/1783.1-93035 ; https://doi.org/10.14711/thesis-991012615767603412 ; http://repository.ust.hk/ir/bitstream/1783.1-93035/1/th_redirect.html

► In recent years, the development of graphene and other two-dimensional (2D) materials, e.g. transition metal dichalcogenides (TMDs), have been experiencing a renaissance since the discovery… (more)

▼ In recent years, the development of graphene and other two-dimensional (2D) materials, e.g. transition metal dichalcogenides (TMDs), have been experiencing a renaissance since the discovery of graphene. These layered materials play increasingly important roles as building blocks for functional devices, due to their versatile physical and chemical properties that can behave as semimetal, semiconductors, metals or superconductors, according to various band gap. In this thesis, firstly, we demonstrate the successful achievement in controlling synthesis of these 2D materials by chemical vapor deposition (CVD) method and reveal the different physical and chemical properties of them with changeable physical structures. By means of tuning the band gap through different strategies, we can expand the applications of them to many promising research fields, e.g. electronics, optoelectronics and energy storage. Specifically, the physical and chemical properties of these 2D materials have been effectively tuned through two approached, including chemical functionalization and heterostructures. In the first part, we have systematically researched the chemical activity differences of few layer graphene (including bilayers and trilayers) through a kinetic dominated chemical functionalization with diazounium salts. Along with the experiment, the intrinsic energy band distribution for few layer graphene with varies stacking modes can contribute to the chemical reaction activity differences is proof-of-principle. Outlined by computational calculations with density functional theory (DFT) as roadmaps, according to the amount of electron in graphene valence band (VB) which can be excited to the conduction band (CB) during chemical reaction for graphene with different stacking modes, their chemical reactivity can be sequenced. In addition, in the second part, the band structure of two different TMDs as semiconductors (n-type MoS₂ and p-type MoTe₂) has been rearranged by forming a vertical heterostructure, resulting in the new optoelectronic property different from either of them. The reshaped band structure for the heterostructures provides a different path for the transfer of photo-excited electrons and resulted in a broadband photo-responsive property which is in stark contrast to the optoelectronic properties of these two TMDs. The approaches demonstrated in this thesis can make the 2D materials become attractive candidates for the fabrication of ultrathin technological devices in next generation of functional materials.

Subjects/Keywords: Chemical vapor deposition ; Graphene ; Spectra ; Synthesis ; Diazo compounds

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APA (6^th Edition):

Ding, Y. C. (2018). Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials. (Thesis). Hong Kong University of Science and Technology. Retrieved from http://repository.ust.hk/ir/Record/1783.1-93035 ; https://doi.org/10.14711/thesis-991012615767603412 ; http://repository.ust.hk/ir/bitstream/1783.1-93035/1/th_redirect.html

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Ding, Yao CBME. “Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials.” 2018. Thesis, Hong Kong University of Science and Technology. Accessed January 20, 2021. http://repository.ust.hk/ir/Record/1783.1-93035 ; https://doi.org/10.14711/thesis-991012615767603412 ; http://repository.ust.hk/ir/bitstream/1783.1-93035/1/th_redirect.html.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Ding, Yao CBME. “Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials.” 2018. Web. 20 Jan 2021.

Vancouver:

Ding YC. Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials. [Internet] [Thesis]. Hong Kong University of Science and Technology; 2018. [cited 2021 Jan 20]. Available from: http://repository.ust.hk/ir/Record/1783.1-93035 ; https://doi.org/10.14711/thesis-991012615767603412 ; http://repository.ust.hk/ir/bitstream/1783.1-93035/1/th_redirect.html.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Ding YC. Physicochemical properties of chemical vapor deposition synthesized two-dimensional functional materials. [Thesis]. Hong Kong University of Science and Technology; 2018. Available from: http://repository.ust.hk/ir/Record/1783.1-93035 ; https://doi.org/10.14711/thesis-991012615767603412 ; http://repository.ust.hk/ir/bitstream/1783.1-93035/1/th_redirect.html

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Iowa State University

29. Adams, Chester Elgin. I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds.

Degree: 1925, Iowa State University

URL: https://lib.dr.iastate.edu/rtd/14201

Subjects/Keywords: Antiseptics; Diazo compounds; Organic Chemistry

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APA (6^th Edition):

Adams, C. E. (1925). I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds. (Thesis). Iowa State University. Retrieved from https://lib.dr.iastate.edu/rtd/14201

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Adams, Chester Elgin. “I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds.” 1925. Thesis, Iowa State University. Accessed January 20, 2021. https://lib.dr.iastate.edu/rtd/14201.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Adams, Chester Elgin. “I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds.” 1925. Web. 20 Jan 2021.

Vancouver:

Adams CE. I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds. [Internet] [Thesis]. Iowa State University; 1925. [cited 2021 Jan 20]. Available from: https://lib.dr.iastate.edu/rtd/14201.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Adams CE. I. Organic oxygen antiseptics, II. The constitution of aliphatic diazo compounds, III. Anti-knock compounds. [Thesis]. Iowa State University; 1925. Available from: https://lib.dr.iastate.edu/rtd/14201

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Texas Tech University

30. Yang, Il-woo. Phase transfer catalytic reactions of aromatic diazonium salts.

Degree: Chemistry, 1981, Texas Tech University

URL: http://hdl.handle.net/2346/10066

Subjects/Keywords: Catalysis; Diazo compounds; Aromatic compounds

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APA · Chicago · MLA · Vancouver · CSE | Export to Zotero / EndNote / Reference Manager

APA (6^th Edition):

Yang, I. (1981). Phase transfer catalytic reactions of aromatic diazonium salts. (Thesis). Texas Tech University. Retrieved from http://hdl.handle.net/2346/10066

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16^th Edition):

Yang, Il-woo. “Phase transfer catalytic reactions of aromatic diazonium salts.” 1981. Thesis, Texas Tech University. Accessed January 20, 2021. http://hdl.handle.net/2346/10066.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7^th Edition):

Yang, Il-woo. “Phase transfer catalytic reactions of aromatic diazonium salts.” 1981. Web. 20 Jan 2021.

Vancouver:

Yang I. Phase transfer catalytic reactions of aromatic diazonium salts. [Internet] [Thesis]. Texas Tech University; 1981. [cited 2021 Jan 20]. Available from: http://hdl.handle.net/2346/10066.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Yang I. Phase transfer catalytic reactions of aromatic diazonium salts. [Thesis]. Texas Tech University; 1981. Available from: http://hdl.handle.net/2346/10066

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

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