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You searched for +publisher:"NSYSU" +contributor:("Chih-Neng Shu"). One record found.

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NSYSU

1. Yu, Yo-Shane. Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms.

Degree: Master, Chemistry, 2011, NSYSU

In this article, we examined different synthetic approaches with varying adding starting materials for the thiol containg schiff-base complex [ZnL1]2(L1=o-C6H4(SH)(CH=NC6H4SH-o)). We found that the key step for successful synthesis of [ZnL1]2 is the formation of zinc aldehyde intermediate. We also break the [ZnL2]2 dimer by adding chelating agent, TMEDA, to obtain the Zn(L1)(TMEDA) monomer. It√Ęs single crystal X-ray structure confirmed, the structure of the target ligand L1. We also synthesized [NiL1]2 by transmetalation of [ZnL1]2 - an easier synthetic approach. We further reduced the imine part on L1 of [ZnL1]2 and Zn(L1)(TMEDA) to get [ZnL2]2(L2=o-C6H4(SH)(CH2NHC6H4SH-o)) and Zn(L2)(TMEDA) respectively for future reactivity studies. Advisors/Committee Members: Tsu-Hsin Chang (chair), Yen-Nan Chiang (committee member), Chih-Neng Shu (chair).

Subjects/Keywords: Thiol; Schiff-Base; Template Synthesis; Transmetalation; Hydrogenation

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APA · Chicago · MLA · Vancouver · CSE | Export to Zotero / EndNote / Reference Manager

APA (6th Edition):

Yu, Y. (2011). Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms. (Thesis). NSYSU. Retrieved from http://etd.lib.nsysu.edu.tw/ETD-db/ETD-search/view_etd?URN=etd-0904111-120521

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Chicago Manual of Style (16th Edition):

Yu, Yo-Shane. “Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms.” 2011. Thesis, NSYSU. Accessed March 26, 2019. http://etd.lib.nsysu.edu.tw/ETD-db/ETD-search/view_etd?URN=etd-0904111-120521.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

MLA Handbook (7th Edition):

Yu, Yo-Shane. “Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms.” 2011. Web. 26 Mar 2019.

Vancouver:

Yu Y. Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms. [Internet] [Thesis]. NSYSU; 2011. [cited 2019 Mar 26]. Available from: http://etd.lib.nsysu.edu.tw/ETD-db/ETD-search/view_etd?URN=etd-0904111-120521.

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

Council of Science Editors:

Yu Y. Synthesis and Characterization of Zinc Schiff-Base Complexes Bearing Sulfur or Nitrogen Donor Atoms. [Thesis]. NSYSU; 2011. Available from: http://etd.lib.nsysu.edu.tw/ETD-db/ETD-search/view_etd?URN=etd-0904111-120521

Note: this citation may be lacking information needed for this citation format:
Not specified: Masters Thesis or Doctoral Dissertation

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