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1.
Sivaswamy, Swetha.
Industrial applications of principles of green chemistry.
Degree: MS, Chemical Engineering, 2012, Georgia Tech
URL: http://hdl.handle.net/1853/44776 
► Cross-linked polyethylene has higher upper use temperature than normal polyethylene and is used as an insulating material for electricity carrying cables and hot water pipes.…
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▼ Cross-linked polyethylene has higher upper use temperature than normal polyethylene and is used as an insulating material for electricity carrying cables and hot water pipes. The most common method of inducing crosslinks is by reaction with silanes. After incorporation of silanes into polyethylene and upon hydrolysis with ambient moisture or with hot water, Si-O-Si crosslinks are formed between the various linear polyethylene chains. Industrially, this reaction is performed routinely. However, the efficiency of this reaction with respect to the silane is low and control of product distribution is difficult. A precise fundamental understanding is necessary to be able to manipulate the reactions and thus, allow for the facile processing of the polymers. Hydrocarbon models of polymers - heptane, dodecane - are being used to study this reaction in the laboratory. For the reaction, vinyltrimethoxysilane is used as the grafting agent along with di-tert-butyl peroxide as the radical initiator. MALDI, a mass spectrometric technique is used for the analysis of the product distribution after work-up. Advanced NMR techniques (COSY, HSQC, DEPT, APT, HMBC) are being conducted on the grafted hydrocarbon compounds to gain an in-depth understanding of the mechanism and regiochemistry of the grafting reaction.
Scalable and cost effective methods to capture CO2 are important to counterbalance some of the global impact of the combustion of fossil fuels on climate change. The main options available now include absorption, adsorption and membrane technology. Amines, especially monoethanolamine, have been the most commercialized technology. However, it is not without disadvantages. House et al have investigated the energy penalty involved in the post-combustion CO2 capture and storage from coal-fired power plants and found that 15-20% reduction in the overall electricity usage is necessary to offset the penalty from capturing and storing 80% of United States coal fleet's CO2 emssions1. Novel non-aqueous amine solvents, developed by the Eckert Liotta group, react with CO2 to form ionic liquids. The ionic liquids readily desorb CO2 upon heating, regenerating the reactive amines and this cycle can be carried out multiple times. An iterative procedure is being adopted to develop amine solvents for CO2 capture. Thermodynamic information like reversal temperature and boiling point of the solvents are collected; they are then used to formulate structure property relationships which allow for new molecules to be engineered. On reaction with CO2, there is a sharp increase in viscosity which is unfavorable from a processing standpoint. Many approaches to mitigate and control viscosity are being studied as well.
1House et al, Energy Environ Sci, 2009, 2, 193-205
Advisors/Committee Members: Dr Charles Eckert (Committee Chair), Dr Charles Liotta (Committee Co-Chair), Dr Amyn Teja (Committee Member).
Subjects/Keywords: Green chemistry; Sustainability; Solvents; Silane grafting; Environmental chemistry Industrial applications; Silane compounds
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APA (6th Edition):
Sivaswamy, S. (2012). Industrial applications of principles of green chemistry. (Masters Thesis). Georgia Tech. Retrieved from http://hdl.handle.net/1853/44776
Chicago Manual of Style (16th Edition):
Sivaswamy, Swetha. “Industrial applications of principles of green chemistry.” 2012. Masters Thesis, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/44776.
MLA Handbook (7th Edition):
Sivaswamy, Swetha. “Industrial applications of principles of green chemistry.” 2012. Web. 15 Jan 2021.
Vancouver:
Sivaswamy S. Industrial applications of principles of green chemistry. [Internet] [Masters thesis]. Georgia Tech; 2012. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/44776.
Council of Science Editors:
Sivaswamy S. Industrial applications of principles of green chemistry. [Masters Thesis]. Georgia Tech; 2012. Available from: http://hdl.handle.net/1853/44776
2.
Esekhile, Omoyemen Edoamen.
Mixed matrix membranes for mixture gas separation of butane isomers.
Degree: PhD, Chemical Engineering, 2011, Georgia Tech
URL: http://hdl.handle.net/1853/42929
► The goal of this project was to understand and model the performance of hybrid inorganic-organic membranes under realistic operating conditions for hydrocarbon gas/vapor separation, using…
(more)
▼ The goal of this project was to understand and model the performance of hybrid inorganic-organic membranes under realistic operating conditions for hydrocarbon gas/vapor separation, using butane isomers as the model vapors and a hybrid membrane of 6FDA-DAM-5A as an advanced separation system.
To achieve the set goal, three objectives were laid out. The first objective was to determine the factors affecting separation performance in dense neat polymer. One main concern was plasticization. High temperature annealing has been reported as an effect means of suppressing plasticization. A study on the effect of annealing temperature was performed by analyzing data acquired via sorption and permeation measurements. Based on the findings from this study, a suitable annealing temperature was determined. Another factor studied was the effect of operating temperature. In deciding a suitable operating temperature, factors such as its possible effect on plasticization as well as reducing heating/cooling cost in industrial application were considered.
Based on the knowledge that industrial applications of this membrane would involve mixture separation, the second objective was to understand and model the complexity of a mixed gas system. This was investigated via permeation measurements using three feed compositions. An interesting transport behavior was observed in the mixed gas system, which to the best of our knowledge, has not been observed in other mixed gas systems involving smaller penetrants. This mixed gas transport behavior presented a challenge in predictability using well-established transport models. Two hypotheses were made to explain the observed transport behavior, which led to the development of a new model termed the HHF model and the introduction of a fitting parameter termed the CAUFFV fit. Both the HHF model and CAUFFV fit showed better agreement with experimental data than the well-established mixed gas transport model.
The final objective was to explore the use of mixed matrix membranes as a means of improving the separation performance of this system. A major challenge with the fabrication of good mixed matrix membranes was the adhesion of the zeolite particle with the polymer. This was addressed via sieve surface modification through a Grignard treatment process. Although a Grignard treatment procedure existed, there was a challenge of reproducibility of the treatment. This challenge was addressed by exploring the relationship between the sieves and the solvent used in the treatment, and taking advantage of this relationship in the Grignard treatment process. This study helped identify a suitable solvent, which allowed for successful and reproducible treatment of commercial LTA sieves; however, treatment of lab-made sieves continues to prove challenging. Based on improved understanding of the Grignard treatment reaction mechanism, modifications were made to the existing Grignard treatment procedure, resulting in the introduction of a "simplified" Grignard treatment procedure. The new procedure…
Advisors/Committee Members: Dr. William Koros (Committee Chair), Dr. Amyn Teja (Committee Member), Dr. Carson Meredith (Committee Member), Dr. Karl Jacob (Committee Member), Dr. Victor Breedveld (Committee Member).
Subjects/Keywords: Mixed matrix membranes; Mixed gas permeation; Butane isomers; Gases Separation; Gas separation membranes; Membranes (Technology); Separation (Technology)
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APA (6th Edition):
Esekhile, O. E. (2011). Mixed matrix membranes for mixture gas separation of butane isomers. (Doctoral Dissertation). Georgia Tech. Retrieved from http://hdl.handle.net/1853/42929
Chicago Manual of Style (16th Edition):
Esekhile, Omoyemen Edoamen. “Mixed matrix membranes for mixture gas separation of butane isomers.” 2011. Doctoral Dissertation, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/42929.
MLA Handbook (7th Edition):
Esekhile, Omoyemen Edoamen. “Mixed matrix membranes for mixture gas separation of butane isomers.” 2011. Web. 15 Jan 2021.
Vancouver:
Esekhile OE. Mixed matrix membranes for mixture gas separation of butane isomers. [Internet] [Doctoral dissertation]. Georgia Tech; 2011. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/42929.
Council of Science Editors:
Esekhile OE. Mixed matrix membranes for mixture gas separation of butane isomers. [Doctoral Dissertation]. Georgia Tech; 2011. Available from: http://hdl.handle.net/1853/42929
3.
Omole, Imona C.
Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams.
Degree: PhD, Chemical Engineering, 2008, Georgia Tech
URL: http://hdl.handle.net/1853/26591
► Natural gas is one of the fastest growing primary energy sources in the world today. The increasing world demand for energy requires increased production of…
(more)
▼ Natural gas is one of the fastest growing primary energy sources in the world today. The increasing world demand for energy requires increased production of high quality natural gas. For the natural gas to be fed into the mainline gas transportation system, it must meet the pipe-line quality standards. Natural gas produced at the wellhead is usually "sub-quality" and contains various impurities such as CO2, H2S, and higher hydrocarbons, which must be removed to meet specifications.
Carbon dioxide is usually the most abundant impurity in natural gas feeds and high CO2 partial pressures in the feed can lead to plasticization, which causes loss of some methane product and may ultimately render the membrane ineffective. Moreover, the presence of highly sorbing higher hydrocarbons in the feed can further reduce membrane performance.
Covalent crosslinking has been shown to increase plasticization resistance in dense films by suppressing the degree of swelling and segmental chain mobility in the polymer, thereby preserving the selectivity of the membrane. This research focuses on extending the dense film success to asymmetric hollow fibers.
In this work, the effect of high pressure CO2 (up to 400 psia CO2 partial pressure) on CO2/CH4 mixed gas separation performance was investigated on defect-free the hollow fiber membrane at different degrees of crosslinking. All the crosslinked fibers were shown to exhibit good resistance to selectivity losses from CO2 induced plasticization, significantly more than the uncrosslinked fibers. Robust resistance of the hollow fiber membranes in the presence of toluene (a highly sorbing contaminant) was also demonstrated as the membranes showed no plasticization. Antiplasticization was found to occur in the presence of toluene feeds with the crosslinkable fibers used in this work.
Advisors/Committee Members: Dr. William J. Koros (Committee Chair), Dr. Amyn Teja (Committee Member), Dr. Christopher W. Jones (Committee Member), Dr. Haskell W. Beckham (Committee Member), Dr. Stephen J. Miller (Committee Member).
Subjects/Keywords: Membrane; Carbon dioxide; Natural gas; Hollow fiber; Polyimide; Gas separation; Gas separation membranes; High pressure (Technology); Natural gas; Crosslinked polymers
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APA (6th Edition):
Omole, I. C. (2008). Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams. (Doctoral Dissertation). Georgia Tech. Retrieved from http://hdl.handle.net/1853/26591
Chicago Manual of Style (16th Edition):
Omole, Imona C. “Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams.” 2008. Doctoral Dissertation, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/26591.
MLA Handbook (7th Edition):
Omole, Imona C. “Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams.” 2008. Web. 15 Jan 2021.
Vancouver:
Omole IC. Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams. [Internet] [Doctoral dissertation]. Georgia Tech; 2008. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/26591.
Council of Science Editors:
Omole IC. Crosslinked polyimide hollow fiber membranes for aggressive natural gas feed streams. [Doctoral Dissertation]. Georgia Tech; 2008. Available from: http://hdl.handle.net/1853/26591
Georgia Tech
4.
Asa-Awuku, Akua Asabea.
The effect of solute dissolution kinetics on cloud droplet formation.
Degree: MS, Chemical Engineering, 2006, Georgia Tech
URL: http://hdl.handle.net/1853/10456
► This study focuses on the importance of solute dissolution kinetics for cloud droplet formation. To comprehensively account for the kinetics, a numerical model of the…
(more)
▼ This study focuses on the importance of solute dissolution kinetics for cloud droplet formation. To comprehensively account for the kinetics, a numerical model of the process was developed. Simulations of cloud droplet growth were performed for solute diffusivity, droplet growth rates, dry particle and droplet diameters relevant for ambient conditions. Simulations suggest that high ambient supersaturations and a decrease in solute diffusivity are major contributors to significant decreases in effective solute surface concentrations. The numerical simulations were incorporated into Khler theory to assess the impact of dissolution kinetics on the droplet equilibrium vapor pressure. For CCN composed of partially soluble material, a significant increase was found in the equilibrium supersaturation of CCN.
Advisors/Committee Members: Dr. Athanasios Nenes (Committee Chair), Dr. Amyn Teja (Committee Member), Dr. Rodney Weber (Committee Member).
Subjects/Keywords: Cloud droplet formation; Activation; Dissolution kinetics; Aerosols; Clouds; Atmosphere, Upper Mathematical models; Drops; Climatology Mathematical models
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APA (6th Edition):
Asa-Awuku, A. A. (2006). The effect of solute dissolution kinetics on cloud droplet formation. (Masters Thesis). Georgia Tech. Retrieved from http://hdl.handle.net/1853/10456
Chicago Manual of Style (16th Edition):
Asa-Awuku, Akua Asabea. “The effect of solute dissolution kinetics on cloud droplet formation.” 2006. Masters Thesis, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/10456.
MLA Handbook (7th Edition):
Asa-Awuku, Akua Asabea. “The effect of solute dissolution kinetics on cloud droplet formation.” 2006. Web. 15 Jan 2021.
Vancouver:
Asa-Awuku AA. The effect of solute dissolution kinetics on cloud droplet formation. [Internet] [Masters thesis]. Georgia Tech; 2006. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/10456.
Council of Science Editors:
Asa-Awuku AA. The effect of solute dissolution kinetics on cloud droplet formation. [Masters Thesis]. Georgia Tech; 2006. Available from: http://hdl.handle.net/1853/10456
Georgia Tech
5.
Williams, Robyn D.
Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform.
Degree: MS, Chemical Engineering, 2005, Georgia Tech
URL: http://hdl.handle.net/1853/7252
► Cirrus clouds cover between 20% - 50% of the globe and are an essential component in the climate. The improved understanding of ice cloud microphysical…
(more)
▼ Cirrus clouds cover between 20% - 50% of the globe and are an essential
component in the climate. The improved understanding of ice cloud
microphysical properties is contingent on acquiring and analyzing in-situ and
remote sensing data from cirrus clouds. In ??u observations of microphysical
properties of ice and mixed-phase clouds using the mini-Video Ice Particle Sizer
(mini-VIPS) aboard robotic unmanned aerial vehicles (UAVs) provide a promising
and powerful platform for obtaining valuable data in a cost-effective, safe, and
long-term manner.
The purpose of this study is to better understand cirrus microphysical
properties by analyzing the effectiveness of the mini-VIPS/UAV in-situ platform.
The specific goals include:
(1) To validate the mini-VIPS performance by comparing the mini-VIPS data
retrieved during an Artic UAV mission with data retrieved from the millimeterwavelength
cloud radar (MMCR) at the Barrow ARM/CART site.
(2) To analyze mini-VIPS data to survey the properties of high latitude mixedphase
clouds
The intercomparison between in-situ and remote sensing measurements
was carried out by comparing reflectivity values calculated from in-situ
measurements with observations from the MMCR facility. Good agreement
between observations and measurements is obtained during the time frame
where the sampled volume was saturated with respect to ice. We also have
1 2
shown that the degree of closure between calculated and observed reflectivity
strongly correlates with the assumption of ice crystal geometry observed in the
mini-VIPS images. The good correlation increases the confidence in mini-VIPS
and MMCR measurements. Finally, the size distribution and ice crystal geometry
obtained from the data analysis is consistent with published literature for similar
conditions of temperature and ice supersaturation.
Advisors/Committee Members: Dr. Athanasios Nenes (Committee Chair), Dr. Amyn Teja (Committee Member), Dr. Judith Curry (Committee Member).
Subjects/Keywords: MMCR; Climate; Cloud; Mini-VIPS; Microphysics; Ice clouds Measurement; Drone aircraft; Clouds Remote sensing; Cloud physics Analysis
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APA ·
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APA (6th Edition):
Williams, R. D. (2005). Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform. (Masters Thesis). Georgia Tech. Retrieved from http://hdl.handle.net/1853/7252
Chicago Manual of Style (16th Edition):
Williams, Robyn D. “Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform.” 2005. Masters Thesis, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/7252.
MLA Handbook (7th Edition):
Williams, Robyn D. “Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform.” 2005. Web. 15 Jan 2021.
Vancouver:
Williams RD. Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform. [Internet] [Masters thesis]. Georgia Tech; 2005. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/7252.
Council of Science Editors:
Williams RD. Studies of Mixed-Phase Cloud Microphysics Using An In-Situ Unmanned Aerial Vehicle (UAV) Platform. [Masters Thesis]. Georgia Tech; 2005. Available from: http://hdl.handle.net/1853/7252
Georgia Tech
6.
Ford, Jackson Walker.
Designing for sustainability with CO2-tunable solvents.
Degree: PhD, Chemical Engineering, 2007, Georgia Tech
URL: http://hdl.handle.net/1853/19866
► Developing greener, more efficient, and less energy-intensive processes will lead the chemical industry into a more sustainable future. Gas-expanded liquids (GXLs) form a unique class…
(more)
▼ Developing greener, more efficient, and less energy-intensive processes will lead the chemical industry into a more sustainable future. Gas-expanded liquids (GXLs) form a unique class of environmentally benign and tunable solvents that can be used in a variety of applications. Through the series of studies presented in this thesis, we have investigated both the properties and applications of GXLs. We have developed a more complete understanding of the interactions between the gas, the organic liquid, and solutes at the molecular level through kinetic and solvatochromic experiments. We have examined a Diels-Alder reaction and an SN2 reaction and have described the kinetic results in terms of intermolecular interactions and local composition enhancement. We have also demonstrated the use of Organic-Aqueous Tunable Solvents, a special case of GXLs, to recycle homogeneous hydroformylation catalysts. The results of this research can be used to guide future applications of GXLs as green reaction solvents.
Advisors/Committee Members: Dr. Charles A. Eckert (Committee Chair), Dr. Charles L. Liotta (Committee Co-Chair), Dr. Amyn Teja (Committee Member), Dr. Dennis W. Hess (Committee Member), Dr. Victor Breedveld (Committee Member).
Subjects/Keywords: Gas-expanded liquids; Alternative solvents; Carbon dioxide; Solvatochromism; Local structure; Carbon dioxide; Solvents; Sustainable engineering; Green products
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APA (6th Edition):
Ford, J. W. (2007). Designing for sustainability with CO2-tunable solvents. (Doctoral Dissertation). Georgia Tech. Retrieved from http://hdl.handle.net/1853/19866
Chicago Manual of Style (16th Edition):
Ford, Jackson Walker. “Designing for sustainability with CO2-tunable solvents.” 2007. Doctoral Dissertation, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/19866.
MLA Handbook (7th Edition):
Ford, Jackson Walker. “Designing for sustainability with CO2-tunable solvents.” 2007. Web. 15 Jan 2021.
Vancouver:
Ford JW. Designing for sustainability with CO2-tunable solvents. [Internet] [Doctoral dissertation]. Georgia Tech; 2007. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/19866.
Council of Science Editors:
Ford JW. Designing for sustainability with CO2-tunable solvents. [Doctoral Dissertation]. Georgia Tech; 2007. Available from: http://hdl.handle.net/1853/19866
Georgia Tech
7.
Janakat, Malina Elizabeth.
Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle.
Degree: PhD, Chemical Engineering, 2006, Georgia Tech
URL: http://hdl.handle.net/1853/10461
► Gas-expanded liquids (GXLs) are a new and benign class of pressure-tunable liquid solvents which show tremendous promise as the next sustainable processing medium. In order…
(more)
▼ Gas-expanded liquids (GXLs) are a new and benign class of pressure-tunable liquid solvents which show tremendous promise as the next sustainable processing medium. In order to realize the potential of GXLs fully, it is necessary to elucidate their cybotactic region and gain an understanding of where properties are different in the bulk and micro-scales and how local structure and order affect both reactions and separations. This work explores the cybotactic region of GXLs and probes the existence and implications of those differences.
This study is started by exploring the cybotactic region of ambient liquid mixtures. Thermodynamic models based on intermolecular forces are used to predict the solubility of multi-functional solids in a variety of solvent mixtures. While this part does not lend any insight into GXLs directly, it acts as a stepping stone in both understanding the intermolecular forces that govern the cybotactic region and by opening the gateway to studying solid solubility in GXLs.
The rest of the study focuses on the differences between bulk and local properties of GXLs. Different probes of polarity in the cybotactic region are compared and the solute dependence of the local structure is explored. Bulk transport properties are measured with different probes in an effort to see if molecular interactions play a role in governing diffusion processes in GXLs.
Advisors/Committee Members: Dr. Charles A. Eckert (Committee Chair), Dr. Charles L. Liotta (Committee Co-Chair), Dr. Amyn Teja (Committee Member), Dr. Rigoberto Hernandez (Committee Member), Dr. William J. Koros (Committee Member).
Subjects/Keywords: Gas-expanded liquids; Cybotactic region
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APA ·
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APA (6th Edition):
Janakat, M. E. (2006). Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle. (Doctoral Dissertation). Georgia Tech. Retrieved from http://hdl.handle.net/1853/10461
Chicago Manual of Style (16th Edition):
Janakat, Malina Elizabeth. “Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle.” 2006. Doctoral Dissertation, Georgia Tech. Accessed January 15, 2021.
http://hdl.handle.net/1853/10461.
MLA Handbook (7th Edition):
Janakat, Malina Elizabeth. “Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle.” 2006. Web. 15 Jan 2021.
Vancouver:
Janakat ME. Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle. [Internet] [Doctoral dissertation]. Georgia Tech; 2006. [cited 2021 Jan 15].
Available from: http://hdl.handle.net/1853/10461.
Council of Science Editors:
Janakat ME. Synergistic Approach to Exploration of the Microstructure of Novel, Tunable Solvents for Reactions, Separations and Catalyst Recycle. [Doctoral Dissertation]. Georgia Tech; 2006. Available from: http://hdl.handle.net/1853/10461
. 
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